Oil solution | 18 ml |
concent of silicone resin | Cs = 50, 67, 75, 80 [wt%] |
ethyl acetate | 1.6 g |
hardening agent | 1.0 g |
surfactant | Span 20 (HLB = 8.6), |
Span 40 (HLB = 6.7), | |
Span 80 (HLB = 4.3) | |
Aqueous solution | 15 ml |
distilled water | 12 ml |
ethanol | 3 ml |
Phase separation condition | |
impeller speed | 5 s−1 |
syringe pump flow rate | 10 ml/h |
Reaction condition | |
temperature | 35˚C |
reaction time | 12 h |
Drying-in-liquid condition | |
temperature | 44˚C |
drying time | 24 h |